71.060.10 - Chemical elements
ICS 71.060.10 Details
Chemical elements
Chemische Elemente
Elements chimiques
Kemični elementi
General Information
This document specifies a thermal pre-ageing procedure for leather to obtain indications about the tendency to the formation of hexavalent chromium under specified conditions and the determination of hexavalent chromium according to ISO 17075-1 or ISO 17075-2.
This thermal pre-ageing procedure does not simulate any real condition in leather production or use.
It is applicable to all types of chromium tanned leather.
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This European Standard defines the specifications and the test methods for carbon black feedstock i.e. coal tar, coal tar fractions or coal tar distillates used for the manufacture of carbon black.
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Applicable to products having As contents equal or more than 0.5 mg/kg. In a well-ventilated cupboard, dissolution of a test portion in carbon tetrachloride. Oxidation of sulphur by bromine and nitric acid. Heating in a boiling water bath to eliminate the exess of bromine, carbon tetrachloride and nitric acid. The analysis is carried out according to ISO 2590. The replacement of some reagents shall be noted.
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Applicable to products having acidities, expressed as H2 SO4 , equal to or more than 0.01 % (m/m). Describes the extraction of acidic substances with a mixture of water and propan-2-ol (isopropyl alcohol). Titration of the extract with standard volumetric sodium hydroxide solution in the presence of phenolphthalein as indicator. The preparation of the sample from the laboratory sample is carried out by grinding a sufficient quantity of the undried material until it passes through a sieve of nominal mesh of 250 m.
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The method is applicable when an agreement has previously been reached between the interested parties for the removal of two representative samples during filling of the tank-wagon at the manufacturer's premises. It cannot be applied when it is intended to determine the water content. The principle consists in checking that the equipment used is gas-tight; collection of the samples in steel bottles. One bottle is intended for the customer and the other is retained by the manufacturer in case an analysis is required for checking purposes. - Replaces ISO Recommendation R 1552-1970.
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Application to products containing at least 98 % of elemental sulphur, expressed as a percentage by mass, of the product dried at 80 °C for 2 h. The difference between the ash and the residue corresponds to the "non-volatile bituminous matter" content at 200 °C. The principle of ashing consists in slow combustion in air of a test portion of the dried product. Heating in a furnace, controlled at 850 °C to 900 °C, and weighing. The determination of non-volatile matter is carried out by slow evaporation in a furnace, controlled at (200 10) °C, in a flow of nitrogen, of the volatile matter and the sulphur. Weighing of the residue after about 10 h.
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Specifies the heating of a test portion in an oven at 80 0C and the determination of the resulting difference in mass by weighing.
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The method relates to the determination of the "volatile water", that which volatilizes at the same time as the chlorine. It is applicable to products having a water content greater than 0,0005 % (m/m). It should not be applied to samples stored in bottles subject to corrosion. The principle consists in absorption of the water by passing the gasified sample into tared absorbers containing phosphorus pentoxide or magnesium perchlorate. Elimination of the gaseous chlorine and volatile impurities by flushing with air or dry nitrogen heated to 80 °C. Absorption of the chlorine in a tared bottle containing sodium hydroxide solution. Weighing of the absorbers to determine, by difference from the original masses, the mass of water.
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The principle consists in sampling of a known volume of chlorine (about 100 ml) obtained by gasification of liquid chlorine. Absorption of the chlorine by a 2% zinc amalgam in the presence of 1 ml of saturated sodium chlorine solution. Measurement of the residual, non-condensable gases such as H2, O2, N2, CO, CO2, etc. Calculation of the volume of chlorine from the difference from total volume, refereed to 100 ml of vaporized sample. The apparatus used is shown diagrammatically in the figure. The safety measures for working with chlorine are listed.
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Is applicable to products having chloride contents, expressed as chlorine, greater than 2 mg/kg. The principle of determination consists in extracting the chlorides by boilling a test portion in aqueous 2-propanol, followed by a quantitative displacement of the thiocyanate ions of mercury(II) thiocynate by the chloride ions contained in an aliquot portion of the extraction solution, and reaction of the thiocyanate ions with iron(III) nitrate to form iron(III) thiocyanate.
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Gives the potentiometric and visual methods als alternatives for the final titration. The principle consists in the combustion of the sulphur in a current of oxygen. Oxidation and fixation of the sulphur dioxide and trioxide gases in chromic and sulphuric acid solutions. Absorption of the carbon dioxide formed in a solution of barium hydroxide, followed by titration in the presence of phenolphthalein and screened methylorange (by xylene cyanol FF) as indicator. Has also been approved by the IUPAC.
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Specifies a method for the determination of the volatile water, that which volatilizes at the same time as the liquid chlorine. It is intended for products with a moisture content of 0,001 % (m/m). The principle consists in contious absorption of the water in the gasified chlorine, flowing at a rate of 100 ml/min over phosphorus pentoxide applied in a thin layer on a glass rod. The glass rod forms an electrolytic cell be means of two electrodes (for example, platinum) wound over its entire length. Decomposition of the water, on absorption. by electrolysis. Measurement of the electrolytic current, which is a function of the water content.
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