Liquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method

This Standard specifies a method, for determining the residual matter in liquefied petroleum gases (LPG), which remains after evaporation at 105 °C. This material represents those products deposited in car LPG vaporizers that are subject to a temperature equal to or greater than the boiling temperature of water. The range of determination extends from 50 mg/kg to 100 mg/kg. Higher concentrations can be determined by adjusting the sample size.
The precision data of the method have been determined from 20 mg/kg to 100 mg/kg, with samples amount from 100 g to 50 g.
This method has been developed as a potential replacement of the commonly used method EN ISO 13757 [1], The advantages of the method are that a small quantity of LPG (100 ml) is required.

Flüssiggas - Bestimmung der gelösten Rückstände - Gravimetrisches Hochtemperaturverfahren

Diese Europäische Norm legt ein Verfahren zur Bestimmung des gelösten Rückstands in Flüssiggas (LPG) fest, der nach der Verdampfung bei 105 °C unter Verwendung des Aufblaseverfahrens nach EN ISO 6246 zurück bleibt.
Der Messbereich reicht von 20 mg/kg bis 100 mg/kg. Höhere Konzentrationen können durch Anpassung der Probenmenge bestimmt werden.
Die Präzisionsdaten des Verfahrens wurden für den Bereich von 20 mg/kg bis 100 mg/kg, mit Probenmengen von 100 g bis 50 g, bestimmt.
ANMERKUNG   Eine alternative Europäische Norm, EN 15470 [1], beschreibt ein gaschromatographisches Verfahren.
WARNUNG - Die Anwendung dieser Norm kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Diese Norm beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieser Norm, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen, und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.

Gaz de pétrole liquéfié - Détermination des résidus dissous - Méthode gravimétrique à haute température

La présente norme européenne spécifie une méthode de détermination des matières résiduelles dissoutes dans le gaz de pétrole liquéfié (GPL) qui subsistent après évaporation à 105 °C avec l’équipement d’évaporation au jet décrit dans l’EN ISO 6246.
L’intervalle de mesure s’étend sur la plage de 20 mg/kg à 100 mg/kg. Des concentrations plus élevées peuvent être mesurées en ajustant la taille de l’échantillon.
Les valeurs de fidélité de cette méthode ont été fixées dans un intervalle de concentration compris entre 20 mg/kg et 100 mg/kg avec des échantillons de 100 g à 50 g.
NOTE   La norme EN 15470 [1] présente une méthode par chromatographie en phase gazeuse.
AVERTISSEMENT - L'utilisation de la présente Norme peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme n'est pas censée aborder tous les problèmes de sécurité concernés par son usage. Il est de la responsabilité des utilisateurs de cette norme de prendre les mesures appropriées pour assurer la sécurité et préserver la santé du personnel avant son application, et pour répondre aux exigences réglementaires et statutaires à cette fin.

Utekočinjeni naftni plini - Določevanje raztopljenih ostankov - Visokotemperaturna gravimetrijska metoda

Ta standard določa metodo za določevanje ostankov snovi v utekočinjenih naftnih plinih (LPG), ki ostanejo po izhlapevanju pri 105 °C. Ta material predstavlja tiste izdelke, ki so naneseni na avtomobilske uparjalnike utekočinjenih naftnih plinov, ki so izpostavljeni temperaturi, enaki ali večji od temperature vrelišča vode. Razpon določanja je 50–100 mg/kg. Višje koncentracije je mogoče določiti s prilagajanjem velikosti vzorca.
Podatki o natančnosti metode so določeni 20–100 mg/kg pri količini vzorca 100–50 g.
Ta metoda je bila razvita kot možna zamenjava običajno uporabljene metode, ki je opisana v standardu EN ISO 13757 [1]. Prednost te metode je v tem, da je potrebna majhna količina (100 ml) utekočinjenega naftnega plina.

General Information

Status
Published
Public Enquiry End Date
03-Jan-2016
Publication Date
06-Sep-2017
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
30-Aug-2017
Due Date
04-Nov-2017
Completion Date
07-Sep-2017

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2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.LVRNRWHPSHUDWXUQDFlüssiggas - Bestimmung der gelösten Rückstände - Gravimetrisches HochtemperaturverfahrenGaz de pétrole liquéfié - Détermination des résidus dissous - Méthode gravimétrique à haute températureLiquefied petroleum gases - Determination of dissolved residues - High-temperature gravimetric method75.160.30Plinska gorivaGaseous fuelsICS:Ta slovenski standard je istoveten z:EN 15471:2017SIST EN 15471:2017en,fr,de01-oktober-2017SIST EN 15471:2017SLOVENSKI
STANDARDSIST EN 15471:20081DGRPHãþD



SIST EN 15471:2017



EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 15471
July
t r s y ICS
y wä s x rä t r Supersedes EN
s w v y sã t r r yEnglish Version
Liquefied petroleum gases æ Determination of dissolved residues æ Highætemperature gravimetric method Gaz de pétrole liquéfié æ Détermination des résidus dissous æ Méthode gravimétrique à haute température Flüssiggas æ Bestimmung der gelösten Rückstände æ Gravimetrisches Hochtemperaturverfahren This European Standard was approved by CEN on
t v April
t r s yä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Avenue Marnix 17,
B-1000 Brussels
9
t r s y CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s w v y sã t r s y ESIST EN 15471:2017



EN 15471:2017 (E) 2 Contents Page European Foreword . 3 1 Scope . 4 2 Normative references . 4 3 Terms and definitions . 4 4 Principle . 4 5 Reagents . 4 6 Apparatus . 5 7 Sampling . 6 8 Procedure. 6 8.1 Apparatus assembling . 6 8.2 Evaporation of the LPG . 7 8.3 Jet evaporation procedure . 7 9 Calculation . 8 10 Expression of results . 8 11 Precision . 8 11.1 General . 8 11.2 Repeatability, r . 8 11.3 Reproducibility, R . 8 Bibliography . 10
SIST EN 15471:2017



EN 15471:2017 (E) 3 European Foreword This document (EN 15471:2017) has been prepared by Technical Committee CEN/TC 19 “Gaseous and liquid fuels, lubricants and related products of petroleum, synthetic and biological origin”, the secretariat of which is held by NEN. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by January 2018, and conflicting national standards shall be withdrawn at the latest by January 2018. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 15471:2007. The changes of this second version compared to the previous version are as follows: a) numerous changes of both technical and editorial nature have been made to add clarity to the text; b) clarification that the use of a drying agent in the desiccator is not recommended; c) the description of the equipment used has been improved; d) a note to filter discs (6.3) was added; e) references to ASTM D381 have been replaced by references to EN ISO 6246. According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 15471:2017



EN 15471:2017 (E) 4 1 Scope This European Standard specifies a method for determining the dissolved residual matter in liquefied petroleum gases (LPG), which remains after evaporation at 105 °C using the jet evaporation equipment described in EN ISO 6246. The measurement range is from 20 mg/kg to 100 mg/kg. Higher concentrations can be determined by adjusting the sample size. The precision data of the method have been determined from 20 mg/kg to 100 mg/kg, with samples amount from 100 g to 50 g. NOTE An alternative European Standard, EN 15470 [1], specifies a gas chromatography method. WARNING — The use of this standard can involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of users of this standard to take appropriate measures to ensure the safety and health of personnel prior to application of the standard, and fulfil statutory and regulatory requirements for this purpose. 2 Normative references The f
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