Gas cylinders - Acetylene cylinders - Basic requirements and type testing (ISO 3807:2013)

This International Standard specifies the basic and type testing requirements for acetylene cylinders with and without fusible plugs with a maximum nominal water capacity of 150 l and requirements regarding production/batch test procedures for manufacturing of acetylene cylinders with porous material. It does not include details of the design of the cylinder shell; these are specified, for example, in ISO 9809-1, ISO 9809-3, ISO 4706 and ISO 7866.

Gasflaschen - Acetylenflaschen - Grundlegende Anforderungen und Baumusterprüfung (ISO 3807:2013)

Dieses Dokument legt die grundlegenden Anforderungen und die Anforderungen an die Baumusterprüfung
von Acetylenflaschen mit und ohne Schmelzsicherungen mit einem maximalen Nennfassungsraum von 150 l
sowie die Anforderungen an die Produktions-/Losprüfverfahren für die Herstellung von Acetylenflaschen mit
porösem Material fest.
Es beinhaltet keine Einzelheiten der Auslegung des Flaschenmantels; diese sind z. B. in ISO 9809-1,
ISO 9809-3, ISO 4706 oder ISO 7866 festgelegt.
ANMERKUNG Die Begrenzung auf 150 l ist von den Normen für die Flaschenmäntel abgeleitet. In der Praxis weisen
Acetylenflaschen jedoch üblicherweise kleinere Fassungsräume als 150 l auf.

Bouteilles à gaz - Bouteilles d'acétylène - Exigences fondamentales et essais de type (ISO 3807:2013)

L'ISO 3807:2013 spécifie les exigences fondamentales et d'essais de type pour les bouteilles d'acétylène avec et sans bouchons fusibles, d'une contenance en eau nominale maximale de 150 l, ainsi que les exigences concernant les modes opératoires d'essai sur lots de production pour la fabrication de bouteilles d'acétylène avec une matière poreuse.
Elle n'inclut pas les caractéristiques de conception de l'enveloppe de la bouteille, celles-ci étant notamment spécifiées dans l'ISO 9809‑1, l'ISO 9809‑3, l'ISO 4706 ou l'ISO 7866.

Plinske jeklenke - Jeklenke za acetilen - Osnovne zahteve in preskus tipa (ISO 3807:2013)

Ta mednarodni standard določa osnovne zahteve in zahteve za preskus tipa za jeklenke za acetilen s stikali za varovalko in brez njih z največjo nominalno vodno kapaciteto 150 l ter zahteve v zvezi s proizvodnimi/serijskimi preskusnimi postopki za proizvodnjo jeklenk za acetilen s poroznim materialom. Ne vključuje podrobnosti o konstruiranju ohišja jeklenke; te podrobnosti so naštete na primer v standardih ISO 9809-1, ISO 9809-3, ISO 4706 in ISO 7866.

General Information

Status
Published
Public Enquiry End Date
31-Aug-2012
Publication Date
17-Nov-2013
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
18-Oct-2013
Due Date
23-Dec-2013
Completion Date
18-Nov-2013

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Standards Content (Sample)

SLOVENSKI STANDARD
SIST EN ISO 3807:2013
01-december-2013
1DGRPHãþD
SIST EN 1800:2007
Plinske jeklenke - Jeklenke za acetilen - Osnovne zahteve in preskus tipa (ISO
3807:2013)
Gas cylinders - Acetylene cylinders - Basic requirements and type testing (ISO
3807:2013)
Gasflaschen - Acetylenflaschen - Grundlegende Anforderungen und Baumusterprüfung
(ISO 3807:2013)
Bouteilles à gaz - Bouteilles d'acétylène - Exigences fondamentales et essais de type
(ISO 3807:2013)
Ta slovenski standard je istoveten z: EN ISO 3807:2013
ICS:
23.020.30 7ODþQHSRVRGHSOLQVNH Pressure vessels, gas
MHNOHQNH cylinders
SIST EN ISO 3807:2013 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.

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SIST EN ISO 3807:2013

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SIST EN ISO 3807:2013


EUROPEAN STANDARD
EN ISO 3807

NORME EUROPÉENNE

EUROPÄISCHE NORM
September 2013
ICS 23.020.30 Supersedes EN 1800:2006
English Version
Gas cylinders - Acetylene cylinders - Basic requirements and
type testing (ISO 3807:2013)
Bouteilles à gaz - Bouteilles d'acétylène - Exigences Gasflaschen - Acetylenflaschen - Grundlegende
fondamentales et essais de type (ISO 3807:2013) Anforderungen und Baumusterprüfung (ISO 3807:2013)
This European Standard was approved by CEN on 3 August 2013.

CEN members are bound to comply with the CEN/CENELEC Internal Regulations which stipulate the conditions for giving this European
Standard the status of a national standard without any alteration. Up-to-date lists and bibliographical references concerning such national
standards may be obtained on application to the CEN-CENELEC Management Centre or to any CEN member.

This European Standard exists in three official versions (English, French, German). A version in any other language made by translation
under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC Management Centre has the same
status as the official versions.

CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and United
Kingdom.





EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION

EUROPÄISCHES KOMITEE FÜR NORMUNG

CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2013 CEN All rights of exploitation in any form and by any means reserved Ref. No. EN ISO 3807:2013: E
worldwide for CEN national Members.

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SIST EN ISO 3807:2013
EN ISO 3807:2013 (E)
Contents Page
Foreword .3
2

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SIST EN ISO 3807:2013
EN ISO 3807:2013 (E)
Foreword
This document (EN ISO 3807:2013) has been prepared by Technical Committee ISO/TC 58 "Gas cylinders" in
collaboration with Technical Committee CEN/TC 23 “Transportable gas cylinders” the secretariat of which is
held by BSI.
This European Standard shall be given the status of a national standard, either by publication of an identical
text or by endorsement, at the latest by March 2014, and conflicting national standards shall be withdrawn at
the latest by March 2014.
Attention is drawn to the possibility that some of the elements of this document may be the subject of patent
rights. CEN [and/or CENELEC] shall not be held responsible for identifying any or all such patent rights.
This document supersedes EN 1800:2006.
This European Standard has been prepared under a mandate given to CEN by the European Commission
and the European Free Trade Association, and supports the objectives of the framework Directives on
Transport of Dangerous Goods.
According to the CEN-CENELEC Internal Regulations, the national standards organizations of the following
countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech
Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece,
Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal,
Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom.
Endorsement notice
The text of ISO 3807:2013 has been approved by CEN as EN ISO 3807:2013 without any modification.

3

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SIST EN ISO 3807:2013

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SIST EN ISO 3807:2013
INTERNATIONAL ISO
STANDARD 3807
Second edition
2013-09-01
Gas cylinders — Acetylene cylinders
— Basic requirements and type testing
Bouteilles à gaz — Bouteilles d’acétylène — Exigences fondamentales
et essais de type
Reference number
ISO 3807:2013(E)
©
ISO 2013

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SIST EN ISO 3807:2013
ISO 3807:2013(E)

COPYRIGHT PROTECTED DOCUMENT
© ISO 2013
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized otherwise in any form
or by any means, electronic or mechanical, including photocopying, or posting on the internet or an intranet, without prior
written permission. Permission can be requested from either ISO at the address below or ISO’s member body in the country of
the requester.
ISO copyright office
Case postale 56 • CH-1211 Geneva 20
Tel. + 41 22 749 01 11
Fax + 41 22 749 09 47
E-mail copyright@iso.org
Web www.iso.org
Published in Switzerland
ii © ISO 2013 – All rights reserved

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SIST EN ISO 3807:2013
ISO 3807:2013(E)

Contents Page
Foreword .iv
Introduction .v
1 Scope . 1
2 Normative references . 1
3 Terms and definitions . 1
4 Basic requirements . 3
4.1 Cylinder shell . 3
4.2 Porous material . 3
4.3 Solvent content and acetylene content . 4
4.4 Working pressure . 4
4.5 Cylinder identification . 4
4.6 Fusible plugs . 4
4.7 Accessories . 5
5 Type approval . 5
5.1 General requirements . 5
5.2 Request for approval . 5
5.3 Cylinder type tests . 6
5.4 Information to be given in the type approval document . 7
6 Manufacturing of the porous material . 8
7 Solvent-free acetylene cylinders . 8
Annex A (normative) Determination of the porosity of the porous material .9
Annex B (normative) Determination of the compressive strength of monolithic
porous materials .10
Annex C (normative) Calculation of the working pressure .11
Annex D (normative) Verification that development of hydraulic pressure is prevented.12
Annex E (normative) Backfire test .14
Annex F (normative) Fire test .18
Annex G (normative) Testing of the integrity of the porous material in the area of joggle welds .21
Annex H (normative) Test procedures for fusible plugs used in acetylene cylinders .22
Annex I (normative) Inspection procedures for the manufacture of acetylene cylinders .24
Annex J (informative) Explanation and examples for the calculation method according to D.3 .26
Bibliography .28
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards
bodies (ISO member bodies). The work of preparing International Standards is normally carried out
through ISO technical committees. Each member body interested in a subject for which a technical
committee has been established has the right to be represented on that committee. International
organizations, governmental and non-governmental, in liaison with ISO, also take part in the work.
ISO collaborates closely with the International Electrotechnical Commission (IEC) on all matters of
electrotechnical standardization.
International Standards are drafted in accordance with the rules given in the ISO/IEC Directives, Part 2.
The main task of technical committees is to prepare International Standards. Draft International
Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies
casting a vote.
Attention is drawn to the possibility that some of the elements of this document may be the subject of
patent rights. ISO shall not be held responsible for identifying any or all such patent rights.
ISO 3807 was prepared by Technical Committee ISO/TC 58, Gas cylinders.
This second edition of ISO 3807 cancels and replaces the first edition of ISO 3807-1:2000 and the first
edition of ISO 3807-2:2000. The main technical modifications are the following:
a) ISO 3807-1 and ISO 3807-2 were revised taking into account EN 1800 and the according requirements
were merged into one standard (ISO 3807).
b) A test for the compressive strength of the porous material was added.
c) A calculation method as an alternative to the elevated temperature test was added.
d) The impact stability test was removed.
e) The procedure for establishing permissible acetylene/solvent concentrations for bundles was
removed and is now included in ISO 13088.
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

Introduction
There are two types of acetylene cylinders operated in certain parts of the world:
— acetylene cylinders with a test pressure of at least 60 bar and without fusible plugs;
— acetylene cylinders with a test pressure of at least 52 bar, fitted with fusible plugs which release the
gas and hence reduce the pressure if the cylinder temperature increases unintentionally.
This International Standard covers the requirements for both types of acetylene cylinders and specifies
specific requirements in separate Annexes.
This International Standard is intended to be used under a variety of national regulatory regimes but has
[1]
been written so that it is suitable for the application of the UN Model Regulations . Attention is drawn to
requirements in the specified relevant national regulations of the country (countries) where the cylinders
are intended to be used that might override the requirements given in this International Standard.
In International Standards, weight is equivalent to a force, expressed in Newton. However, in common
parlance (as used in terms defined in this International Standard), the word “weight” continues to be
used to mean “mass”, even though this practice is deprecated (ISO 80000-4).
In this International Standard the unit bar is used, due to its universal use in the field of technical gases.
It should, however, be noted that bar is not an SI unit, and that the according SI unit for pressure is Pa.
Pressure values given in this International Standard are given as gauge pressure (pressure exceeding
atmospheric pressure) unless noted otherwise.
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SIST EN ISO 3807:2013

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SIST EN ISO 3807:2013
INTERNATIONAL STANDARD ISO 3807:2013(E)
Gas cylinders — Acetylene cylinders — Basic requirements
and type testing
1 Scope
This International Standard specifies the basic and type testing requirements for acetylene cylinders with
and without fusible plugs with a maximum nominal water capacity of 150 l and requirements regarding
production/batch test procedures for manufacturing of acetylene cylinders with porous material.
It does not include details of the design of the cylinder shell; these are specified, for example, in
ISO 9809-1, ISO 9809-3, ISO 4706 and ISO 7866.
NOTE The limitation to 150 l is derived from the definition for cylinder in the UN Model Regulations. However,
in practice acetylene cylinders in general have lower water capacities than 150 l.
2 Normative references
The following referenced documents are indispensable for the application of this document. For dated
references, only the edition cited applies. For undated references, the latest edition of the referenced
document (including any amendments) applies.
ISO 10297, Gas cylinders — Cylinder valves — Specification and type testing
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
3.1
acetylene cylinder
cylinder, manufactured and suitable for the transport of acetylene, containing a porous material (3.6) and
solvent (3.9) (where applicable) for acetylene with a valve and other accessories affixed to the cylinder
Note 1 to entry: For solvent-free acetylene cylinders, see Clause 7.
Note 2 to entry: When there is no risk of ambiguity, the word “cylinder” is used.
3.2
cylinder shell
empty cylinder, manufactured and suitable for receiving and containing a porous
material (3.6) for use as part of an acetylene cylinder (3.1)
3.3
fusible plug
non-reclosing pressure relief device designed to function by the yielding or melting of a plug of fusible
material at a predetermined temperature
3.4
manufacturer
company responsible for filling the cylinder shell (3.2) with porous material (3.6)
and which generally prepares it for the first charge of acetylene
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

3.5
maximum acetylene content
specified maximum weight of acetylene including saturation acetylene (3.8) in an
acetylene cylinder (3.1)
Note 1 to entry: When using tare S, the maximum acetylene charge may be used. The maximum acetylene charge
is the maximum acetylene content minus the saturation acetylene.
3.6
porous material
single or multiple component material introduced to or formed in the cylinder
shell (3.2), that, due its porosity, allows the absorption of a solvent/acetylene solution
Note 1 to entry: The porous material can be either monolithic, consisting of a solid product typically obtained by
reacting materials or by materials connected together with a binder, or non-monolithic, consisting of granular,
fibrous or similar materials without addition of a binder.
3.7
porosity
ratio of the total volume [water capacity (3.13)] of the cylinder shell (3.2) minus
the volume of the solid fraction (portion) of the porous material (3.6), to the water capacity (3.13) of the
cylinder shell (3.2)
Note 1 to entry: For the determination of the porosity see Annex A or Annex I.
3.8
saturation acetylene
acetylene dissolved in the solvent (3.9) in the acetylene cylinder (3.1) at atmospheric
pressure (1,013 bar) and at a temperature of 15 °C
3.9
solvent
liquid that is absorbed by the porous material (3.6) and is capable of dissolving
and releasing acetylene
Note 1 to entry: The following abbreviations are used: “A” for acetone and “DMF” for dimethylformamide.
3.10
specified solvent content
weight of solvent (3.9) that the acetylene cylinder (3.1) shall contain that is
established during prototype testing
3.11
tare
reference weight of the acetylene cylinder (3.1) including the specified solvent
content (3.10)
Note 1 to entry: The tare is further specified in accordance with 3.11.1 to 3.11.3.
Note 2 to entry: For acetylene cylinders with solvent, the tare is expressed by indicating either tare S or both,
tare A and tare S. For solvent-free acetylene cylinders, the tare is expressed by indicating tare F. For the tare used
for acetylene cylinders in bundles, see ISO 13088.
3.11.1
tare A
sum of the weights of the empty cylinder shell (3.2), the porous material (3.6), the
specified solvent content (3.10), the valve, the coating and the valve guard, where applicable, and all other
parts which are permanently attached to the acetylene cylinder (3.1) when it is presented to be filled
Note 1 to entry: Generally valve guards are included in the tare and are considered to be permanently attached
(and are not removed when the cylinder is filled). This, however, might not always be the case.
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

3.11.2
tare S
tare A (3.11.1) plus the weight of the saturation acetylene (3.8)
3.11.3
tare F
tare A (3.11.1) minus the specified solvent content (3.10)
3.12
top clearance
gap between the inside of the cylinder shoulder and the monolithic porous
material (3.6)
3.13
water capacity
actual capacity of the cylinder shell (3.2) measured by filling the cylinder shell
(3.2) with water
Note 1 to entry: The cylinder shell is defined as being empty of any porous material; see 3.2.
3.14
working pressure
settled pressure at a uniform reference temperature of 15 °C in an acetylene
cylinder (3.1) containing the specified solvent content (3.10) and the maximum acetylene content (3.5)
Note 1 to entry: For the determination of the working pressure see Annex C.
4 Basic requirements
4.1 Cylinder shell
The acetylene cylinder shell shall conform to the requirements of the relevant International Standard
for design and construction of the cylinders, e.g.
— for seamless steel, ISO 9809-1, ISO 9809-3;
— for welded steel, ISO 4706;
— for seamless aluminium alloy, ISO 7866.
NOTE Other standards for the design and construction of cylinders are in preparation and appropriate
standards should be conformed to when published.
The minimum test pressure for acetylene cylinders without fusible plugs shall be 60 bar.
The minimum test pressure for acetylene cylinders with fusible plugs shall be 52 bar.
4.2 Porous material
The porous material shall be compatible with the cylinder shell, the solvent and acetylene and shall
not form dangerous or harmful products with these. For common porous materials consisting of inert
materials (e.g. calcium silicate hydrate), this is generally the case.
The maximum specified porosity shall not exceed the minimum specified porosity by more than 3 %
when determined in accordance with Annex A.
P − P ≤ 3 %
max min
(1)
where P is the porosity of the porous material, in %.
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

The compressive strength as determined in accordance with Annex B shall be at least 2 MPa (20 bar).
For safety reasons, the porous material shall be able to prevent the propagation of an acetylene
decomposition within the cylinder and shall be of such quality that it enables the acetylene cylinder to
meet the requirements of Annex D and Annex E.
Acetylene cylinders equipped with fusible plugs shall pass the fire test described in Annex F in addition.
Where cylinder shells with joggle welds are used, it shall be verified that the welds do not damage the
porous material in accordance with Annex G.
To ensure the quality and uniform distribution of the porous material in the acetylene cylinder and
the quality and amount of the solvent, test procedures shall be established by the manufacturer of the
porous material in accordance with Annex I.
4.3 Solvent content and acetylene content
The solvent shall be compatible with the cylinder shell. For the commonly used solvents acetone and
DMF this is generally the case.
The specified solvent content and the maximum acetylene content for an acetylene cylinder shall be
such that the cylinder will meet the requirements specified in Annex D and Annex E.
The specified solvent content and the maximum acetylene content for an acetylene cylinder equipped with
fusible plugs shall be such that the cylinder will meet the requirements specified in Annex F in addition.
4.4 Working pressure
When the cylinder has been filled with the specified solvent content and the maximum acetylene content,
and the pressure has reached equilibrium at a uniform reference temperature of 15 °C, the gauge pressure
in the cylinder shall not exceed the working pressure as calculated in accordance with Annex C.
4.5 Cylinder identification
For the stamp marking of acetylene cylinders see the relevant regulations. Further information can be
found in ISO 13769.
In addition, solvent free acetylene cylinders shall bear the words “solvent-free” painted in a clear and
visible manner.
NOTE Attention is drawn to requirements for marking in relevant regulations that might override the
requirements given in this International Standard.
4.6 Fusible plugs
For acetylene cylinders equipped with fusible plugs, the fusible plugs shall be sized and selected as to
location and quantity so that the fusible plug(s) are capable of preventing bursting of the normally filled
cylinder when subjected to a fire test in accordance with Annex F.
The fusible plug shall utilize a fusible alloy having a yield temperature between 98 °C and 110 °C. The
yield temperature is the temperature at which the fusible alloy becomes sufficiently soft to extrude
from its holder to permit discharge of acetylene.
The fusible alloy may be installed in a threaded steel or brass plug. The threaded plug shall be fitted into
a boss or pad, preferably on the cylinder top or in the cylinder valve. Bottom plugs are not permitted for
cylinders used in bundles.
The fusible plugs shall be sample tested for yield temperature and for resistance to extrusion and
leakage as a quality control procedure during manufacture and prior to installation into the cylinder in
accordance with Annex H.
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

4.7 Accessories
Valves for use with acetylene cylinders shall conform to the requirements of ISO 10297. Other accessories
should conform to the requirements of appropriate International Standards, where available, e.g. valve
guards and caps according to ISO 11117.
5 Type approval
5.1 General requirements
Representative cylinders, selected according to 5.3.1, by or on behalf of the approving body, shall
successfully withstand the type tests as required in 5.3.2 prior to type approval being granted to the
manufacturer of the porous material.
5.2 Request for approval
5.2.1 Range of an approval
A request for approval of acetylene cylinders may cover a range of different cylinder water capacities
provided that:
a) the cylinder shells are made from the same type of material (steel or aluminium alloy);
b) the construction of the cylinder shells is similar (either seamless cylinders or cylinders with
circumferential joggle welds or cylinders with butt welds only);
c) the nominal outside diameter of the cylinders falls within the range of either:
— ≤ 270 mm, or
— > 270 mm;
d) the cylinders contain the same porous material from the same factory and the same solvent;
e) the specified solvent content per litre water capacity of the cylinder shell is the same;
f) the maximum acetylene content per litre water capacity of the cylinder shell is the same.
NOTE The maximum acetylene content per litre water capacity may be lower than the value approved,
provided the solvent content is not changed.
5.2.2 Information to be supplied
Each request for approval shall include the following information:
a) General information, including the following information:
— identification (trade name) of the porous material to be stamped on the cylinder;
— name of the manufacturer and place of production of the porous material.
b) Information on the different types of acetylene cylinders which form the subject of the request for
approval and which includes, for each cylinder water capacity, the following information:
— nominal (minimum guaranteed) water capacity in litres;
— test pressure of the cylinder shell in bar;
— working pressure at 15 °C in bar;
— solvent to be used;
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SIST EN ISO 3807:2013
ISO 3807:2013(E)

— specified solvent content in kilograms per litre cylinder water capacity;
— maximum acetylene content in kilograms per litre cylinder water capacity;
— number and location of the fusible plugs, if applicable.
c) A description of the porous material as it exists in the cylinder, which gives sufficient information
concerning production process and quality control procedures (see Annex I). The description shall
include the following:
— maximum top clearance, which shall be consistent with periodic inspection rejection criteria;
— core hole size and packing material, where applicable.
d) A report on the porosity determinations carried out by, or on behalf of, the manufacturer according
to the method given in Annex A and the nominal porosity and tolerance within which the porous
material is to be manufactured.
e) A report on the co
...

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