SIST EN 1431:2018
(Main)Bitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation
Bitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation
This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions. The method can also be used to obtain residue and oil distillate for further testing. NOTE The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use.
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels Destillation
Diese Europäische Norm legt ein Verfahren zur quantitativen Bestimmung des verbleibenden Bindemittels und des Öldestillates in Bitumenemulsionen fest.
Das Verfahren kann auch angewendet werden, um den Rückstand und das Öldestillat für weitere Prüfungen zu erhalten.
ANMERKUNG Die an dem mit diesem Verfahren gewonnenen Material ermittelten Stoffeigenschaften gleichen nicht notwendigerweise denen der Ausgangsstoffe, aus denen die Emulsion hergestellt wurde; dies gilt besonders für polymermodifizierte Bitumen, verschnittene und gefluxte bitumenhaltige Bindemittel.
WARNUNG - Die Anwendung dieser Norm kann die Anwendung gefährlicher Stoffe, Arbeitsgänge und Geräte mit sich bringen. Diese Norm beansprucht nicht, alle damit verbundenen Sicherheitsprobleme zu behandeln. Es liegt in der Verantwortung des Anwenders dieser Norm, vor ihrer Anwendung geeignete Maßnahmen für die Sicherheit und den Gesundheitsschutz des Personals zu ergreifen und dafür Sorge zu tragen, dass behördliche und gesetzliche Maßnahmen eingehalten werden.
Bitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitume
La présente Norme européenne définit une méthode de détermination quantitative du liant résiduel et du distillat d'huile dans des émulsions bitumineuses.
La présente méthode d'essai peut également être utilisée pour obtenir du liant résiduel et du distillat d'huile pour des essais ultérieurs.
NOTE Les propriétés du matériau récupéré par le présent essai ne sont pas nécessairement les mêmes que celles des matériaux d'origine à partir desquels on a produit l'émulsion, et ce plus particulièrement pour les bitumes modifiés par des polymères, les bitumes fluidifiés et les bitumes fluxés.
AVERTISSEMENT - L'utilisation de la présente Norme européenne peut impliquer l'intervention de produits, d'opérations et d'équipements à caractère dangereux. La présente Norme européenne n’est pas censée aborder tous les problèmes de sécurité associés à son usage. Il est de la responsabilité de l'utilisateur de consulter et d'établir des règles de sécurité et d'hygiène appropriées et de déterminer l'applicabilité des restrictions réglementaires avant utilisation.
Bitumen in bitumenska veziva - Določevanje veziva in oljnega destilata v bitumenskih emulzijah z metodo destilacije
Ta evropski standard določa metodo za kvantitativno določevanje veziva in oljnega destilata v bitumenskih emulzijah. Metoda se lahko uporablja tudi za pridobivanje ostankov in oljnega destilata za nadaljnje preskušanje. OPOMBA: Lastnosti materiala, pridobljenega v preskusih, niso nujno enake lastnostim izvirnih materialov, iz katerih je bila emulzija izdelana. To še posebej velja za bitumne, modificirane s polimeri. OPOZORILO – Pri uporabi tega standarda so lahko prisotni nevarni materiali, postopki in oprema. Ta standard ne obravnava vseh varnostnih težav, ki se nanašajo na njegovo uporabo. Za vzpostavitev ustreznih varnostnih in zdravstvenih praks ter za določitev uporabnosti regulativnih omejitev pred uporabo je odgovoren uporabnik tega standarda.
General Information
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Standards Content (Sample)
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels DestillationBitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat d'huile dans les émulsions de bitumeBitumen and bituminous binders - Determination of residual binder and oil distillate from bitumen emulsions by distillation91.100.50Veziva. Tesnilni materialiBinders. Sealing materials75.140Voski, bitumni in drugi naftni proizvodiWaxes, bituminous materials and other petroleum productsICS:Ta slovenski standard je istoveten z:EN 1431:2018SIST EN 1431:2018en,fr,de01-junij-2018SIST EN 1431:2018SLOVENSKI
STANDARDSIST EN 1431:20091DGRPHãþD
SIST EN 1431:2018
EUROPEAN STANDARD NORME EUROPÉENNE EUROPÄISCHE NORM
EN 1431
March
t r s z ICS
y wä s v râ
{ sä s r rä w r Supersedes EN
s v u sã t r r {English Version
Bitumen and bituminous binders æ Determination of residual binder and oil distillate from bitumen emulsions by distillation Bitumes et liants bitumineux æ Détermination par distillation du liant résiduel et du distillat d 5huile dans les émulsions de bitumes
Bitumen und bitumenhaltige Bindemittel æ Bestimmung des Destillationsrückstandes und des Öldestillates von Bitumenemulsionen mittels Destillation This European Standard was approved by CEN on
x November
t r s yä
egulations which stipulate the conditions for giving this European Standard the status of a national standard without any alterationä Upætoædate lists and bibliographical references concerning such national standards may be obtained on application to the CENæCENELEC Management Centre or to any CEN memberä
translation under the responsibility of a CEN member into its own language and notified to the CENæCENELEC Management Centre has the same status as the official versionsä
CEN members are the national standards bodies of Austriaá Belgiumá Bulgariaá Croatiaá Cyprusá Czech Republicá Denmarká Estoniaá Finlandá Former Yugoslav Republic of Macedoniaá Franceá Germanyá Greeceá Hungaryá Icelandá Irelandá Italyá Latviaá Lithuaniaá Luxembourgá Maltaá Netherlandsá Norwayá Polandá Portugalá Romaniaá Serbiaá Slovakiaá Sloveniaá Spainá Swedená Switzerlandá Turkey and United Kingdomä
EUROPEAN COMMITTEE FOR STANDARDIZATION COMITÉ EUROPÉEN DE NORMALISATION EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre:
Rue de la Science 23,
B-1040 Brussels
9
t r s z CEN All rights of exploitation in any form and by any means reserved worldwide for CEN national Membersä Refä Noä EN
s v u sã t r s z ESIST EN 1431:2018
EN 1431:2018 (E) 2 Contents Page European foreword . 3 1 Scope . 4 2 Normative references . 4 3 Terms and definitions . 4 4 Principle . 5 5 Reagents and materials . 5 6 Apparatus . 5 7 Sampling . 6 8 Procedure. 6 9 Calculation . 8 10 Expression of results . 8 11 Precision . 8 11.1 Repeatability . 8 11.2 Reproducibility . 8 12 Test report . 9 Annex A (informative)
Characteristics of thermometer . 14 Bibliography . 15
SIST EN 1431:2018
EN 1431:2018 (E) 3 European foreword This document (EN 1431:2018) has been prepared by Technical Committee CEN/TC 336 “Bituminous binders”, the secretariat of which is held by AFNOR. This European Standard shall be given the status of a national standard, either by publication of an identical text or by endorsement, at the latest by September 2018, and conflicting national standards shall be withdrawn at the latest by September 2018. Attention is drawn to the possibility that some of the elements of this document may be the subject of patent rights. CEN shall not be held responsible for identifying any or all such patent rights. This document supersedes EN 1431:2009. The main technical changes are: — Clause 3.2: since EN 13808:2013 now clearly refers to residual binder after distillation, the NOTE is no longer necessary and has thus been discarded. — Clause 5.2: alternative basic solutions to sodium hydroxide are allowed. — Clause 6.3: electric ring heater, which may be coupled to a temperature sensor, is described as another possible way for applying heat. This equipment may only be used if the purpose of the test is to determine residual binder and oil distillate content, without the determination of residual binder properties. — Clause 6.6: mercury stem thermometers are replaced by temperature measuring devices allowing similar temperature determinations to be made. Annex A (characteristics of mercury stem thermometer) becomes informative. — Clause 8.5: when electrical heating is used, the total distillation process may be extended to 120 min. — Clauses 8.6 and 8.8: at the end of the distillation procedure, the residue is to be cooled down whatever the next steps. If the residual binder is to be further used for the preparation of test samples, it is to be reheated in accordance to EN 12594 (and not to 260 °C as in EN 1431:2009). — Clause 9 and 10: as for residual binder content, oil distillate content is to be expressed as a mass percentage. Alternative methods to EN ISO 3838 or values provided by the supplier may be used for the determination of oil distillate density. According to the CEN-CENELEC Internal Regulations, the national standards organisations of the following countries are bound to implement this European Standard: Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia, Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania, Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Serbia, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and the United Kingdom. SIST EN 1431:2018
EN 1431:2018 (E) 4 1 Scope This European Standard specifies a method for the quantitative determination of residual binder and oil distillate in bituminous emulsions. The method can also be used to obtain residue and oil distillate for further testing. NOTE The properties of the material recovered in the test are not necessarily the same as those of the original materials from which the emulsion was produced, especially for polymer modified bitumens, cut-back and fluxed bituminous binders. WARNING — The use of this standard may involve hazardous materials, operations and equipment. This standard does not purport to address all of the safety problems associated with its use. It is the responsibility of the user of this standard to establish appropriate safety and health practices and determine the applicability of regulatory limitations prior to use. 2 Normative references The following documents are referred to in the text in such a way that some or all of their content constitutes requirements of this document. For dated references, only the edition cited applies. For undated references, the latest edition of the referenced document (including any amendments) applies. EN 58, Bitumen and bituminous binders — Sampling bituminous binders EN 573-3, Aluminium and aluminium alloys — Chemical composition and form of wrought products — Part 3: Chemical composition and form of products EN 1425, Bitumen and bituminous binders — Characterization of perceptible properties EN 12594, Bitumen and bituminous binders — Preparation of test samples ISO 565, Test sieves — Metal wire cloth, perforated metal plate and electroformed sheet — Nominal sizes of openings EN ISO 3838, Crude petroleum and liquid or solid petroleum products — Determination of density or relative density — Capillary-stoppered pyknometer and graduated bicapillary pyknometer methods (ISO 3838) EN ISO 4788, Laboratory glassware — Graduated measuring cylinders (ISO 4788) 3 Terms and definitions For the purposes of this document, the following terms and definitions apply. ISO and IEC maintain terminological databases for use in standardization at the following addresses: — IEC Electropedia: available at http://www.electropedia.org/ — ISO Online browsing platform: available at http://www.iso.org/obp 3.1 oil distillate hydrocarbon fraction which is distilled and collected in the graduated cylinder under conditions specified in this test SIST EN 1431:2018
EN 1431:2018 (E) 5 3.2 residual binder after distillation residue from a bituminous emulsion after distillation of water and oil distillate Note 1 to entry: The amount of the residual binder after distillation (% by mass) is referred to as the “residual binder content” of the emulsion. 3.3 binder content of the emulsion sum of residual binder content and oil distillate content 4 Principle Water and oil distillate are distilled from the bituminous emulsion, and separated in a graduated cylinder, leaving a residue of residual binder. 5 Reagents and materials 5.1 Cleaning agents, as used conventionally in a laboratory. 5.2 Sodium hydroxide solution 40 g/l, or other suitable basic solution. 6 Apparatus Usual laboratory apparatus and glassware, together with the following: 6.1 Aluminium alloy still (see Figure 1) or iron still, (241 ± 5) mm in height by (100 ± 2) mm external diameter with a (3,2 ± 0,2) mm thickness wall. Lid (see Figure 1) of suitable dimensions to allow two temperature measuring devices (6.6) to be inserted through a stopper and an outlet of suitable diameter to enabl
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SLOVENSKI STANDARD
oSIST prEN 1431:2016
01-april-2016
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Bitumen and bituminous binders - Determination of residual binder and oil distillate from
bitumen emulsions by distillation
Bitumen und bitumenhaltige Bindemittel - Bestimmung des Destillationsrückstandes und
des Öldestillates von Bitumenemulsionen mittels Destillation
Bitumes et liants bitumineux - Détermination par distillation du liant résiduel et du distillat
d'huile dans les émulsions de bitume
Ta slovenski standard je istoveten z: prEN 1431
ICS:
75.140 Voski, bitumni in drugi naftni Waxes, bituminous materials
proizvodi and other petroleum products
91.100.50 Veziva. Tesnilni materiali Binders. Sealing materials
oSIST prEN 1431:2016 en,fr,de
2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.
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oSIST prEN 1431:2016
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oSIST prEN 1431:2016
DRAFT
EUROPEAN STANDARD
prEN 1431
NORME EUROPÉENNE
EUROPÄISCHE NORM
February 2016
ICS 75.140; 91.100.50 Will supersede EN 1431:2009
English Version
Bitumen and bituminous binders - Determination of
residual binder and oil distillate from bitumen emulsions
by distillation
Bitumes et liants bitumineux - Détermination par Bitumen und bitumenhaltige Bindemittel -
distillation du liant résiduel et du distillat d'huile dans Destillationsrückstands und des Oldestillates von
les émulsions de bitume Bitumenemulsionen mittels Destillation
This draft European Standard is submitted to CEN members for enquiry. It has been drawn up by the Technical Committee
CEN/TC 336.
If this draft becomes a European Standard, CEN members are bound to comply with the CEN/CENELEC Internal Regulations
which stipulate the conditions for giving this European Standard the status of a national standard without any alteration.
This draft European Standard was established by CEN in three official versions (English, French, German). A version in any other
language made by translation under the responsibility of a CEN member into its own language and notified to the CEN-CENELEC
Management Centre has the same status as the official versions.
CEN members are the national standards bodies of Austria, Belgium, Bulgaria, Croatia, Cyprus, Czech Republic, Denmark, Estonia,
Finland, Former Yugoslav Republic of Macedonia, France, Germany, Greece, Hungary, Iceland, Ireland, Italy, Latvia, Lithuania,
Luxembourg, Malta, Netherlands, Norway, Poland, Portugal, Romania, Slovakia, Slovenia, Spain, Sweden, Switzerland, Turkey and
United Kingdom.
Recipients of this draft are invited to submit, with their comments, notification of any relevant patent rights of which they are
aware and to provide supporting documentation.
Warning : This document is not a European Standard. It is distributed for review and comments. It is subject to change without
notice and shall not be referred to as a European Standard.
EUROPEAN COMMITTEE FOR STANDARDIZATION
COMITÉ EUROPÉEN DE NORMALISATION
EUROPÄISCHES KOMITEE FÜR NORMUNG
CEN-CENELEC Management Centre: Avenue Marnix 17, B-1000 Brussels
© 2016 CEN All rights of exploitation in any form and by any means reserved Ref. No. prEN 1431:2016 E
worldwide for CEN national Members.
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oSIST prEN 1431:2016
prEN 1431:2016 (E)
Contents Page
European foreword . 3
1 Scope . 4
2 Normative references . 4
3 Terms and definitions . 4
4 Principle . 4
5 Reagents and materials . 5
6 Apparatus . 5
7 Sampling . 6
8 Procedure. 6
9 Calculation . 7
10 Expression of results . 7
11 Precision . 8
11.1 Repeatability . 8
11.2 Reproducibility . 8
12 Test report . 8
Annex A (informative) Characteristics of thermometer . 12
Bibliography . 13
2
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oSIST prEN 1431:2016
prEN 1431:2016 (E)
European foreword
This document (prEN 1431:2016) has been prepared by Technical Committee CEN/TC 336 “Bituminous
binders”, the secretariat of which is held by AFNOR.
This document is currently submitted to the CEN Enquiry.
This document will supersede EN 1431:2009.
3
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oSIST prEN 1431:2016
prEN 1431:2016 (E)
1 Scope
This European Standard specifies a method for the quantitative determination of residual binder and oil
distillate in bituminous emulsions.
The method can also be used to obtain residue and oil distillate for further testing.
NOTE The properties of the material recovered in the test are not necessarily the same as those of the
original materials from which the emulsion was produced, especially for polymer modified bitumens, cut-back
and fluxed bituminous binders.
WARNING — The use of this standard may involve hazardous materials, operations and
equipment. This standard does not purport to address all of the safety problems associated with
its use. It is the responsibility of the user of this standard to establish appropriate safety and
health practices and determine the applicability of regulatory limitations prior to use.
2 Normative references
The following documents, in whole or in part, are normatively referenced in this document and are
indispensable for its application. For dated references, only the edition cited applies. For undated
references, the latest edition of the referenced document (including any amendments) applies.
EN 58, Bitumen and bituminous binders - Sampling bituminous binders
EN 1425, Bitumen and bituminous binders - Characterization of perceptible properties
EN 12594, Bitumen and bituminous binders - Preparation of test samples
ISO 565, Test sieves — Metal wire cloth, perforated metal plate and electroformed sheet — Nominal sizes
of openings
EN ISO 4788, Laboratory glassware - Graduated measuring cylinders (ISO 4788)
3 Terms and definitions
For the purposes of this document, the following terms and definitions apply.
3.1
oil distillate
hydrocarbon fraction which is distilled and collected in the graduated cylinder under conditions
specified in this test
3.2
residual binder by distillation
residue from a bituminous emulsion after distillation of water and oil distillate
4 Principle
Water and oil distillate are distilled from the bituminous emulsion, and separated in a graduated
cylinder, leaving a residue of residual binder.
4
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oSIST prEN 1431:2016
prEN 1431:2016 (E)
5 Reagents and materials
5.1 Cleaning agents, as used conventionally in a laboratory.
5.2 Sodium hydroxide solution 40 g/l, or other suitable basic solution.
6 Apparatus
6.1 Aluminium alloy still (see Figure 1) or iron still, (241 ± 5) mm in height by (101 ± 1) mm external
diameter with a (3,2 ± 0,2) mm thickness wall and a (125 ± 5) mm inside diameter ring burner, having
holes on the inner circumference and having three appropriate spacers or guide pins, to ensure centring
of burner around the still (see Figure 2).
Lid (see Figure 1) of suitable dimensions to allow two temperature measuring devices (6.4) to be
inserted through a stopper and an outlet of suitable diameter to enable connection tube to be connected
also through a stopper.
NOTE All tolerances in 6.1 and shown on Figure 1 and Figure 2 are production tolerances for the
manufactures of the test equipment. No calibration/verification concerning these tolerances is valid in Quality
Control.
The ring burner may be replaced by any alternative means of heating provided the same specified
temperature and distillation conditions are achieved. In the event of a dispute, the reference ring
burner as heating apparatus shall be used.
6.2 Connection apparatus, consisting of a g
...
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