Graphic technology -- Process control -- Certified reference material for opaque area calibration of transmission densitometers

This International Standard defines requirements for a half-tone certified reference material which may be used for the opaque area percentage calibration of transmission densitometers or colorimeters for use in the graphic arts.
This International Standard is not applicable to the calibration of transmission densitometers in terms of ISO standard diffuse density.
NOTE Test methods for determining the opaque area percentage are given in the informative annex A.

Technologie graphique -- Maîtrise de procédé -- Matériel de référence certifié pour la calibration des densitomètres transmission en pourcentage de superficie opaque

Grafična tehnologija – Procesni nadzor – Certificiran referenčni material za umerjanje opačnih površin na transmisijskih denziometrih

General Information

Status
Published
Publication Date
31-Dec-2004
Technical Committee
Current Stage
6060 - National Implementation/Publication (Adopted Project)
Start Date
01-Jan-2005
Due Date
01-Jan-2005
Completion Date
01-Jan-2005

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INTERNATIONAL ISO
STANDARD 12645
First edition
1998-11-01
Graphic technology — Process control —
Certified reference material for opaque area
calibration of transmission densitometers
Technologie graphique — Maîtrise de procédé — Matériel de référence
certifié pour la calibration des densitomètres transmission en pourcentage
de superficie opaque
A
Reference number
ISO 12645:1998(E)

---------------------- Page: 1 ----------------------
ISO 12645:1998(E)
Foreword
ISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISO
member bodies). The work of preparing International Standards is normally carried out through ISO technical
committees. Each member body interested in a subject for which a technical committee has been established has
the right to be represented on that committee. International organizations, governmental and non-governmental, in
liaison with ISO, also take part in the work. ISO collaborates closely with the International Electrotechnical
Commission (IEC) on all matters of electrotechnical standardization.
Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.
Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.
International Standard ISO 12645 was prepared by Technical Committee ISO/TC 130, Graphic technology.
Annexes A to E of this International Standard for information only.
©  ISO 1998
All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronic
or mechanical, including photocopying and microfilm, without permission in writing from the publisher.
International Organization for Standardization
Case postale 56 • CH-1211 Genève 20 • Switzerland
Internet iso@iso.ch
Printed in Switzerland
ii

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©
ISO ISO 12645:1998(E)
Introduction
In the graphic arts, the modulation of transmittance or reflectance is often achieved by printing half-tones rather than
continuous tones, as would be the case in photography.
The process control of the generation and transfer of half-tone patterns is essential to the graphic arts industry. For
the process control of transmission type material one monitors the percentage of the total area that is virtually
opaque. Measurements are carried out on well-defined half-tone control patches which contain regularly-spaced,
circular half-tone dots. The measuring instrument is either a densitometer or a colorimeter of the spectrophotometer
or tristimulus type. The opaque area percentage is usually set equal to the ratio of the relative transmittance factors
of the half-tone and that of the solid. With densitometers one calculates the transmittance factors from the ISO
standard diffuse (opal) densities, the corresponding expression for the ratio has been given by Murray and Davies,
see [E.2] and equations (1) and (2) of clause 3.
In principle, the opaque area percentage for positive-polarity films should be identical to the tone value as defined in
the graphic arts; for negative-polarity films it should be identical to 100 % minus the tone value. In reality, however,
there may be errors which produce small deviations between the two quantities; there is thus a need for an
independent check on the determination of the tone value by densitometers and colorimeters.
In the graphic arts process chain, particularly important steps are "image setting", "film duplication" and
"platemaking". During these steps, there is no highly diffusive medium present which could be compared to the
opal-glass diffuser of densitometers according to ISO 5-2 [E.3]. It would thus appear that the opal-glass instrument
is not the best solution for graphic arts applications. However, the opal-glass design permits a relatively simple
construction; such instruments are widely used in the graphic arts industry.
When calibrating a densitometer with a stepped density reference material (at least two steps), usually both the zero
point and the slope factor are adjusted. The latter is the ratio of the density difference between the steps as read by
the densitometer and the density difference as reported by a national standardizing laboratory. If the ratio deviates
from 1, the base of the logarithm used for converting transmittance factor into transmittance factor density is not 10
as required by definition. As a consequence, the tone values calculated from the densities may deviate from the
opaque area percentages. It is important to note that the (absolute) ISO standard diffuse density calibration of a
densitometer may be dependent on the thickness of the sample. The stepped density reference material used for
the density calibration should therefore have the same thickness as the samples to be measured, otherwise only
relative densities can be measured. For many graphic arts applications, however, absolute density measurements
are not the issue but the control of the opaque area percentage of half-tone film. This quantity determines the size
of image elements, such as half-tone dots or lines, produced by transfer steps such as film duplication and
platemaking. The densitometer is then zeroed on the clear film and the densities of a half-tone and a solid are
measured. The Murray-Davies-formula, [E.2] and equations (1) and (2) of clause 3, is used to determine tone
values from the density values, see also ISO 12647-1.
It is known that transmission densitometers of the opal type are subject to multiple oblique-angle interreflections
between the opal and the surfaces close to it, see ISO 5-2 [E.3]. These include the two surfaces of the sample and
those on the side of the instrument opposing the opal. For samples of low density, reflections from all those
surfaces may contribute to the efflux measured at the back of the opal. At (absolute) ISO standard diffuse densities
near zero, the densities read by an opal instrument are thus slightly lower than those of a diffuse sphere type
instrument; 0,03 is a typical difference. This effect has to be taken into account if transmission densities or
reflectance factors read by instruments of different design are compared. For samples of higher densities, the
reflections from all surfaces but the surface next to the opal are effectively suppressed. During the measurement of
a half-tone pattern, the latter influences the interreflection effect in two ways: The image elements may have a
reflectance different from the film base, they also tend to attenuate reflections from surfaces further removed from
the opal. Therefore, the tone values determined from densities measured with an opal instrument may differ from
the actual opaque area percentage of the sample which can be determined by microscopic measurement or by a
sphere type instrument (which does not show the interreflection effect).
ISO 12647-1 specifies that transmission densities shall be measured by instruments complying to ISO 5-2, thus
there can be no ambiguity when quoting (absolute) ISO standard diffuse densities such as clear film densities.
iii

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©
ISO 12645:1998(E) ISO
The interreflection effect can be artificially attenuated if the opal is kept at a distance of, say, 25 mm from the
measured object. Another method is to place a neutral filter with a density of at least 0,3 between the opal and the
sample. The filter tends to attenuate the light coming back from the opal towards the sample and also the
reflections.
The interreflection effect may produce a discrepancy of typically 3 % between the tone value of a half-tone as
determined with a transmission densitometer of the opal type and the opaque area percentage as determined from
independent measurements of the dot pattern. The discrepancy cannot be circumvented by proper zeroing or
adjustment of the slope factor of the instrument, it depends on the magnitude of the opaque area percentage. Thus
there is a need for an independent check on the tone value determination by a transmission densitometer and, if
necessary, the establishment of a table that converts tone values into opaque area percentages. This International
Standard specifies requirements for two types of reference materials that provide half-tone control patches with dot
patterns of accurately defined dimensions that may serve as "Certified reference materials" (CRM) if the
1)
requirements of ISO 15790 are also fulfilled.
Reference materials may be produced from half-tone film material or a thin glass slab with a chromium deposit. The
latter's advantages are a very small fringe width, a wavelength-independent attenuation and a good uniformity of
opaque area percentage over the control patch. The thickness, the scattering properties and the wavelength
dependence of the transmission density differ from those of graphic arts film material. It might thus be suspected
that this invalidates the use of such a reference material as a standard. It has been shown, however, that thickness
changes of less than 1 mm shift only the zero point of a densitometer, thus the densitometric opaque area
percentage calculation is not affected. Other test series showed that interposing films of varying scattering
properties between the chromium/glass reference material and the opal did not affect the opaque area percentage
determination, within the measurement accuracy. The absence of a wavelength dependence can be regarded as an
asset: Since the wavelength dependencies of graphic arts films differ much from each other, there is no established
dependence that could be used for such a reference material.
___________
1)  See informative annex E.
iv

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©
INTERNATIONAL STANDARD  ISO ISO 12645:1998(E)
Graphic technology — Process control — Certified reference
material for opaque area calibration of transmission densitometers
1 Scope
This International Standard defines requirements for a half-tone certified reference material which may be used for
the opaque area percentage calibration of transmission densitometers or colorimeters for use in the graphic arts.
This International Standard is not applicable to the calibration of transmission densitometers in terms of ISO
standard diffuse density.
NOTE Test methods for determining the opaque area percentage are given in the informative annex A.
2 Normative reference
The following normative document contains provisions which, through reference in this text, constitute provisions of
this International Standard. For dated references, subsequent amendments to, or revisions of, any of these
publications do not apply. However, parties to agreements based on this International Standard are encouraged to
investigate the possibility of applying the most recent edition of the normative document indicated below. For
undated references, the latest edition of the normative document referred to applies. Members of ISO and IEC
maintain registers of currently valid International Standards.
ISO 12647-1:1996, Graphic technology — Process control for the manufacture of half-tone colour separations,
proof and production prints — Part 1: Parameters and measurement methods.
3 Definitions
For the purposes of this International Standard, the definitions given in CIE 17.4 and the following apply. They are
given in alphabetical order.
NOTE For quantities, the preferred unit is given together with the definition. By definition, the unit of formerly so-called
“dimensionless quantities” is 1.
3.1
control patch
area produced for control and measurement purposes
[ISO 12647-1]
3.2
core density
transmission density in the centre of an isolated opaque image element such as a half-tone dot or line
Unit: 1
[ISO 12647-1]
3.3
fringe width (of an isolated opaque image element)
average distance between the density contour lines corresponding to 10 % and 90 % of the minimum core density
specified for the printing process under consideration
Unit: μm
[ISO 12647-1]
1

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©
ISO 12645:1998(E) ISO
3.4
opaque area percentage
P
percentage of total area that is nearly opaque to radiation in the wavelength range of interest
3.5
polarity (of a transmission object)
positive if clear and solid areas on the object correspond to unprinted and solid areas on the print, respectively.
Negative if clear and solid areas on the object correspond to solid and unprinted areas on the print, respectively
3.6
screen ruling
screen frequency
f
number of image elements, such as dots or lines, per length in the direction which produces the largest number
-1
Unit: cm
[ISO 12647-1]
3.7
screen width
reciprocal of screen frequency
Unit: cm
[ISO 12647-1]
3.8
tone value
dot area (on a transmission object of positive polarity)
A
percentage calculated from the formula:
−−()DD
t0
11− 0
=−100%%⋅100 . . . (1)
A
−−()DD
s0
11− 0
where
D is the transmission density of the clear substrate;
0
D is the transmission density of the solid;
s
D is the transmission density of the half-tone.
t
[ISO 12647-1]
NOTE Also known as film printing dot area.
3.9
tone value
dot area (on a half-tone object of negative polarity)
A
percentage calculated from the formula:
−−()DD
t0
11− 0
A=−100%%⋅100 . . . (2)
−−()DD
s0
11− 0
where
D is the transmission density of the clear substrate;
0
D is the transmission density of the solid;
s
D is the transmission density of the half-tone.
t
[ISO 12647-1]
NOTE Also known as film printing dot area.
2

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©
ISO ISO 12645:1998(E)
4 Requirements
4.1 Materials
The substrate shall consist of a clear material with a pattern of opaque half-tone dots on one side. At normal
incid
...

2003-01.Slovenski inštitut za standardizacijo. Razmnoževanje celote ali delov tega standarda ni dovoljeno.Technologie graphique -- Maîtrise de procédé -- Matériel de référence certifié pour la calibration des densitomètres transmission en pourcentage de superficie opaqueGraphic technology -- Process control -- Certified reference material for opaque area calibration of transmission densitometers37.100.01VSORãQRGraphic technology in generalICS:Ta slovenski standard je istoveten z:ISO 12645:1998SIST ISO 12645:2005en01-januar-2005SIST ISO 12645:2005SLOVENSKI
STANDARD



SIST ISO 12645:2005



AReference numberISO 12645:1998(E)INTERNATIONALSTANDARDISO12645First edition1998-11-01Graphic technology — Process control —Certified reference material for opaque areacalibration of transmission densitometersTechnologie graphique — Maîtrise de procédé — Matériel de référencecertifié pour la calibration des densitomètres transmission en pourcentagede superficie opaqueSIST ISO 12645:2005



ISO 12645:1998(E)©
ISO 1998All rights reserved. Unless otherwise specified, no part of this publication may be reproduced or utilized in any form or by any means, electronicor mechanical, including photocopying and microfilm, without permission in writing from the publisher.International Organization for StandardizationCase postale 56 · CH-1211 Genève 20 · SwitzerlandInternetiso@iso.chPrinted in SwitzerlandiiForewordISO (the International Organization for Standardization) is a worldwide federation of national standards bodies (ISOmember bodies). The work of preparing International Standards is normally carried out through ISO technicalcommittees. Each member body interested in a subject for which a technical committee has been established hasthe right to be represented on that committee. International organizations, governmental and non-governmental, inliaison with ISO, also take part in the work. ISO collaborates closely with the International ElectrotechnicalCommission (IEC) on all matters of electrotechnical standardization.Draft International Standards adopted by the technical committees are circulated to the member bodies for voting.Publication as an International Standard requires approval by at least 75 % of the member bodies casting a vote.International Standard ISO 12645 was prepared by Technical Committee ISO/TC 130, Graphic technology.Annexes A to E of this International Standard for information only.SIST ISO 12645:2005



© ISOISO 12645:1998(E)iiiIntroductionIn the graphic arts, the modulation of transmittance or reflectance is often achieved by printing half-tones rather thancontinuous tones, as would be the case in photography.The process control of the generation and transfer of half-tone patterns is essential to the graphic arts industry. Forthe process control of transmission type material one monitors the percentage of the total area that is virtuallyopaque. Measurements are carried out on well-defined half-tone control patches which contain regularly-spaced,circular half-tone dots. The measuring instrument is either a densitometer or a colorimeter of the spectrophotometeror tristimulus type. The opaque area percentage is usually set equal to the ratio of the relative transmittance factorsof the half-tone and that of the solid. With densitometers one calculates the transmittance factors from the ISOstandard diffuse (opal) densities, the corresponding expression for the ratio has been given by Murray and Davies,see [E.2] and equations (1) and (2) of clause 3.In principle, the opaque area percentage for positive-polarity films should be identical to the tone value as defined inthe graphic arts; for negative-polarity films it should be identical to 100 % minus the tone value. In reality, however,there may be errors which produce small deviations between the two quantities; there is thus a need for anindependent check on the determination of the tone value by densitometers and colorimeters.In the graphic arts process chain, particularly important steps are "image setting", "film duplication" and"platemaking". During these steps, there is no highly diffusive medium present which could be compared to theopal-glass diffuser of densitometers according to ISO 5-2 [E.3]. It would thus appear that the opal-glass instrumentis not the best solution for graphic arts applications. However, the opal-glass design permits a relatively simpleconstruction; such instruments are widely used in the graphic arts industry.When calibrating a densitometer with a stepped density reference material (at least two steps), usually both the zeropoint and the slope factor are adjusted. The latter is the ratio of the density difference between the steps as read bythe densitometer and the density difference as reported by a national standardizing laboratory. If the ratio deviatesfrom 1, the base of the logarithm used for converting transmittance factor into transmittance factor density is not 10as required by definition. As a consequence, the tone values calculated from the densities may deviate from theopaque area percentages. It is important to note that the (absolute) ISO standard diffuse density calibration of adensitometer may be dependent on the thickness of the sample. The stepped density reference material used forthe density calibration should therefore have the same thickness as the samples to be measured, otherwise onlyrelative densities can be measured. For many graphic arts applications, however, absolute density measurementsare not the issue but the control of the opaque area percentage of half-tone film. This quantity determines the sizeof image elements, such as half-tone dots or lines, produced by transfer steps such as film duplication andplatemaking. The densitometer is then zeroed on the clear film and the densities of a half-tone and a solid aremeasured. The Murray-Davies-formula, [E.2] and equations (1) and (2) of clause 3, is used to determine tonevalues from the density values, see also ISO 12647-1.It is known that transmission densitometers of the opal type are subject to multiple oblique-angle interreflectionsbetween the opal and the surfaces close to it, see ISO 5-2 [E.3]. These include the two surfaces of the sample andthose on the side of the instrument opposing the opal. For samples of low density, reflections from all thosesurfaces may contribute to the efflux measured at the back of the opal. At (absolute) ISO standard diffuse densitiesnear zero, the densities read by an opal instrument are thus slightly lower than those of a diffuse sphere typeinstrument; 0,03 is a typical difference. This effect has to be taken into account if transmission densities orreflectance factors read by instruments of different design are compared. For samples of higher densities, thereflections from all surfaces but the surface next to the opal are effectively suppressed. During the measurement ofa half-tone pattern, the latter influences the interreflection effect in two ways: The image elements may have areflectance different from the film base, they also tend to attenuate reflections from surfaces further removed fromthe opal. Therefore, the tone values determined from densities measured with an opal instrument may differ fromthe actual opaque area percentage of the sample which can be determined by microscopic measurement or by asphere type instrument (which does not show the interreflection effect).ISO 12647-1 specifies that transmission densities shall be measured by instruments complying to ISO 5-2, thusthere can be no ambiguity when quoting (absolute) ISO standard diffuse densities such as clear film densities.SIST ISO 12645:2005



ISO 12645:1998(E)© ISOivThe interreflection effect can be artificially attenuated if the opal is kept at a distance of, say, 25 mm from themeasured object. Another method is to place a neutral filter with a density of at least 0,3 between the opal and thesample. The filter tends to attenuate the light coming back from the opal towards the sample and also thereflections.The interreflection effect may produce a discrepancy of typically 3 % between the tone value of a half-tone asdetermined with a transmission densitometer of the opal type and the opaque area percentage as determined fromindependent measurements of the dot pattern. The discrepancy cannot be circumvented by proper zeroing oradjustment of the slope factor of the instrument, it depends on the magnitude of the opaque area percentage. Thusthere is a need for an independent check on the tone value determination by a transmission densitometer and, ifnecessary, the establishment of a table that converts tone values into opaque area percentages. This InternationalStandard specifies requirements for two types of reference materials that provide half-tone control patches with dotpatterns of accurately defined dimensions that may serve as "Certified reference materials" (CRM) if therequirements of ISO 157901) are also fulfilled.Reference materials may be produced from half-tone film material or a thin glass slab with a chromium deposit. Thelatter's advantages are a very small fringe width, a wavelength-independent attenuation and a good uniformity ofopaque area percentage over the control patch. The thickness, the scattering properties and the wavelengthdependence of the transmission density differ from those of graphic arts film material. It might thus be suspectedthat this invalidates the use of such a reference material as a standard. It has been shown, however, that thicknesschanges of less than 1 mm shift only the zero point of a densitometer, thus the densitometric opaque areapercentage calculation is not affected. Other test series showed that interposing films of varying scatteringproperties between the chromium/glass reference material and the opal did not affect the opaque area percentagedetermination, within the measurement accuracy. The absence of a wavelength dependence can be regarded as anasset: Since the wavelength dependencies of graphic arts films differ much from each other, there is no establisheddependence that could be used for such a reference material.___________1)
See informative annex E.SIST ISO 12645:2005



INTERNATIONAL STANDARD
© ISOISO 12645:1998(E)1Graphic technology — Process control — Certified referencematerial for opaque area calibration of transmission densitometers1 ScopeThis International Standard defines requirements for a half-tone certified reference material which may be used forthe opaque area percentage calibration of transmission densitometers or colorimeters for use in the graphic arts.This International Standard is not applicable to the calibration of transmission densitometers in terms of ISOstandard diffuse density.NOTE
Test methods for determining the opaque area percentage are given in the informative annex A.2 Normative referenceThe following normative document contains provisions which, through reference in this text, constitute provisions ofthis International Standard. For dated references, subsequent amendments to, or revisions of, any of thesepublications do not apply. However, parties to agreements based on this International Standard are encouraged toinvestigate the possibility of applying the most recent edition of the normative document indicated below. Forundated references, the latest edition of the normative document referred to applies. Members of ISO and IECmaintain registers of currently valid International Standards.ISO 12647-1:1996, Graphic technology — Process control for the manufacture of half-tone colour separations,proof and production prints — Part 1: Parameters and measurement methods.3 DefinitionsFor the purposes of this International Standard, the definitions given in CIE 17.4 and the following apply. They aregiven in alphabetical order.NOTE
For quantities, the preferred unit is given together with the definition. By definition, the unit of formerly so-called“dimensionless quantities” is 1.3.1control patcharea produced for control and measurement purposes[ISO 12647-1]3.2core densitytransmission density in the centre of an isolated opaque image element such as a half-tone dot or lineUnit: 1[ISO 12647-1]3.3fringe width (of an isolated opaque image element)average distance between the density contour lines corresponding to 10 % and 90 % of the minimum core densityspecified for the printing process under considerationUnit: µm[ISO 12647-1]SIST ISO 12645:2005



ISO 12645:1998(E)© ISO23.4opaque area percentagePpercentage of total area that is nearly opaque to radiation in the wavelength range of interest3.5polarity (of a transmission object)positive if clear and solid areas on the object correspond to unprinted and solid areas on the print, respectively.Negative if clear and solid areas on the object correspond to solid and unprinted areas on the print, respectively3.6screen rulingscreen frequencyfnumber of image elements, such as dots or lines, per length in the direction which produces the largest numberUnit: cm-1[ISO 12647-1]3.7screen widthreciprocal of screen frequencyUnit: cm[ISO 12647-1]3.8tone valuedot area (on a transmission object of positive polarity)Apercentage calculated from the formula:ADDDD=---×----100100%%110110()()t0s0. . . (1)whereD0is the transmission density of the clear substrate;Dsis the transmission density of the solid;Dtis the transmission density of the half-tone.[ISO 12647-1]NOTE
Also known as film printing dot area.3.9tone valuedot area
...

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